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Copper bis(thiosemicarbazone) Complexes with Pendent Polyamines: Effects of Proton Relays and Charged Moieties on Electrocatalytic HER

https://doi.org/10.1002/ejic.202000774

Calvary, Caleb A. ; Hietsoi, Oleksandr ; Hofsommer, Dillon T. ; Brun, Henry C. ; Costello, Alison M. ; Mashuta, Mark S. ; Spurgeon, Joshua M. ; Buchanan, Robert M. ; Grapperhaus, Craig A. ( January 2021 , European Journal of Inorganic Chemistry)
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Photocatalytic hydrogen evolution on Si photocathodes modified with bis(thiosemicarbazonato)nickel( ii )/Nafion

https://doi.org/10.1039/c9cc04117f

Gulati, Saumya ; Hietsoi, Oleksandr ; Calvary, Caleb A. ; Strain, Jacob M. ; Pishgar, Sahar ; Brun, Henry C. ; Grapperhaus, Craig A. ; Buchanan, Robert M. ; Spurgeon, Joshua M. ( August 2019 , Chemical Communications)

The molecular catalyst diacetyl-bis( N -4-methyl-3-thiosemi-carbazonato)nickel( ii ) (NiATSM) was integrated with Si for light-driven hydrogen evolution from water. Compared to an equivalent loading of Ni metal, the NiATSM/p-Si electrode performed better. Durability of the surface-bound catalyst under operation in acid was achieved without covalent attachment by using Nafion binding.
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Synthesis, Characterization, and HER Activity of Pendant Diamine Derivatives of NiATSM: Synthesis, Characterization, and HER Activity of Pendant Diamine Derivatives of NiATSM

https://doi.org/10.1002/ejic.201900721

Calvary, Caleb A. ; Hietsoi, Oleksandr ; Strain, Jacob M. ; Mashuta, Mark S. ; Spurgeon, Joshua M. ; Buchanan, Robert M. ; Grapperhaus, Craig A. ( August 2019 , European Journal of Inorganic Chemistry)